Capillary Columns High-Performance Columns
SH-I-5MS Low-polarity phase: Crossbond™ 5% diphenyl / 95% dimethyl polysiloxane Tested and guaranteed for ultra-low bleed; improved signal-to-noise ratio for better sensitivity and mass spectral integrity. General-purpose columns for semi-volatiles, phenols, amines, residual solvents, drugs of abuse, pesticides, PCB congeners (e.g., Aroclor mixes), solvent impurities.
SH-I-5MS Structure
Equivalent to USP G27 and G36 phases.
Similar phases: HP-5ms UI, HP-5ms, DB-5, Ultra-2, CP Sil 8 CB, SPB-5, Equity-5
ID
df
Temp. Range
20 m
25 m
50 m
0.18 µm
-60 to 330/350 °C
227-36015-01
−
−
0.18 mm
0.30 µm
-60 to 330/350 °C
227-36016-01
−
−
0.36 µm
-60 to 330/350 °C
227-36017-01
−
−
0.20 mm 0.33 µm
-60 to 330/350 °C
−
227-36018-01
227-36018-02
ID
df
Temp. Range
15 m
30 m
60 m
0.25 µm
-60 to 330/350 °C
221-75940-15
221-75940-30
227-36019-01
0.40 µm
-60 to 330/350 °C
−
227-36020-01
−
0.25 mm
0.50 µm
-60 to 330/350 °C
227-36021-01
221-75941-30
221-75942-60
1.00 µm
-60 to 330/350 °C
227-36022-01
227-36022-02
227-36022-03
0.25 µm
-60 to 330/350 °C
227-36023-01
221-75943-30
227-36023-02
0.32 mm
0.50 µm
-60 to 330/350 °C
227-36024-01
221-75944-30
227-36024-02
1.00 µm
-60 to 330/350 °C
227-36025-01
227-36025-02
227-36025-03
0.25 µm
-60 to 330/350 °C
227-36026-01
227-36026-02
−
0.50 µm
-60 to 330/350 °C
227-36027-01
227-36027-02
−
0.53 mm
1.00 µm
-60 to 330/350 °C
227-36028-01
227-36028-02
−
1.50 µm
-60 to 330/350 °C
227-36029-01
227-36029-02
−
Peaks 1. Chloroneb 2. Pentachlorobenzene 3. alpha-BHC
GC Multiresidue Pesticide
21. cis -Chlordane 22. trans -Nonachlor 23. Chlorfenson (Ovex) 24. 4,4'-DDE 25. Dieldrin 26. 2,4'-DDD 27. Endrin 28. Ethylan (Perthane) 29. Endosulfan II
4. Hexachlorobenzene 5. Pentachloroanisole 6. beta-BHC 7. gamma-BHC (Lindane) 8. delta-BHC 9. Endosulfan ether 10. Heptachlor 11. Pentachlorothioanisole 12. Aldrin 13. 4,4'-Dichlorobenzophenone 14. Fenson 15. Isodrin 16. Heptachlor epoxide (Isomer B) 17. Chlorbenside 18. trans -Chlordane 19. 2,4'-DDE 20. Endosulfan I
30. 4,4'-DDD 31. 2,4'-DDT 32. cis -Nonachlor 33. Endrin aldehyde 34. 4,4'-Methoxychlor olefin 35. Endosulfan sulfate 36. 4,4'-DDT 37. 2,4'-Methoxychlor 38. Endrin ketone 39. Tetradifon 40. Mirex
Conditions
Column
: SH-I-5MS, 30 m, 0.25 mm ID, 0.25 um (P/N: 221-75940-30) : 1 μL split (split ratio 50:1)
Inj. Vol.
Inj. Temp
: 250 °C
Oven Temp
: 90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min) : He, constant flow rate 1.4 mL/min
Carrier Gas
Detector
: MS-QP Transfer Line Temp: 290 °C Source Temp: 325 °C Solvent Delay Time: 5 min Ionization: EI
Pg C-7
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