GC Columns
Analysis of Organic Solvents
22
21
57
6
37
3
23
15
47
69
18
16
43
11 9
8
66
33,34
20 19
64
2
40,41
56
46
17
32
10
63
45
30
25
52 53
7
73
62
24 26
35 36 38 39
59
50
45
1
14
71 72
44
12
75
27
42
49
58
60
55
70
28
67 68
65
74
31
29
61
54
51
48
13
Peaks 1. Methanol 2. Ethanol 3. Acetaldehyde + Ethyl Ether 4. 1,1-Dichloroethylene 5. Isopropanol
27. 1,2-Dimethoxyethane 28. Ethylene Glycol Monomethyl Ether
52. Methyl Butyl Ketone 53. Cyclohexanol 54. 1,1,2,2-Tetrachloroethane 55. Isoamyl Acetate 56. Butyl Acrylate 57. Ethylene Glycol Monobutyl Ether 58. Anisole + Propylene Glycol Monomethyl Ether Acetate 59. n-Amyl Acetate 60. Ethylene Glycol Monoethyl Ether Acetate 61. N,N-Dimethylformamide 62. Isooctanol 63. Cyclohexanone 64. o-Dichlorobenzene 65. Diethylene Glycol Monoethyl Ether 66. Benzyl Alcohol 67. N,N-Dimethylacetamide 68. Dimethyl Sulfoxide 69. Tetralin 70. Diethylene Glycol Monobutyl Ether
29. Ethylenechlorohydrin 30. Methyl Ethyl Ketone 31. Nitromethane 32. Propylene Glycol Monomethyl Ether + Isopropyl Acetate 33. Ethyl Acrylate 34. Isoamyl Alcohol 35. Methyl Methacrylate 36. Ethylene Glycol Monoethyl Ether 37. Toluene 38. 1,4-Dioxane 39. tetrachloroethylene
6. Dichloromethane + Hexane 7. trans-1,2-Dichloroethylene 8. tert.-Butanol 9. tert.-Butyl Methyl Ether 10. Isopropyl Ether 11. n-Propanol 12. Ethyl Formate 13. Chloroform 14. Methyl Acetate 15. Cyclohexane 16. Tetrachloromethane + sec.-Butanol 17. Isooctane 18. Isobutanol + 1,1,1-Trichloroethane
40. n-Propyl Acetate 41. n-Amyl Alcohol 42. Epichlorohydrin 43. Pyridine 44. Ethylene Glycol Monoisopropyl Ether 45. Isobutyl Acetate 46. Methyl Isobutyl Ketone + Ethylbenzene 47. Chlorobenzene
19. Acetonitrile 20. Acrylonitrile 21. Benzene
71. 2-Ethylhexyl Acrylate 72. N-Methylpyrrolidone 73. Isophorone 74. 1,3-Dimethyl-2-Imidazolidinone 75. Sulfolane
48. p-Xylene 49. m-Xylene 50. n-Butyl Acetate 51. o-Xylene
22. Tetrahydrofuran + methylcyclohexane 23. Methyl Acrylate + 1,2-Dichloroethane 24. Trichloroethylene 25. n-Butanol 26. Ethyl Acetate
Conditions
Instrument
: GC-2010
Column Injection Inj. Temp
: SH-200, 60 m, 0.32 mm ID, 1.00 μm (P/N: 227-36186-02)
: Split (split ratio: 50:1)
: 250 °C
Carrier Gas Oven Temp
: He, constant linear velocity mode, 25 cm/sec
: 40 °C (0 min) to 310 °C at 4 °C/min
Detector
: FID, 330 °C
Pg C-24
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