Capillary Columns Dedicated Columns
SH-1614 5% diphenyl / 95% dimethyl polysiloxane
Optimized for PBDE analysis by EPA Method 1614.
Short column option resolves BDE-209 three times faster, with less thermal breakdown.
Unique deactivation gives higher BDE-209 response than competitor columns, for greater analytical sensitivity.
Exceeds EPA Method 1614 resolution criteria for BDE-49 and BDE-71.
ID
df
Temp. Range
15 m
30 m
0.25 mm 0.10 µm
-60 to 330/360 °C
227-36265-01
227-36265-02
Brominated Flame Retardants
Peaks 1. BDE-10 2. BDE-7 3. BDE-8 4. BDE-11 5. BDE-12 6. BDE-13 7. BDE-15 8. BDE-30 9. BDE-32 10. BDE-17 11. BDE-25 12. BDE-28 13. BDE-33 14. BDE-35
15. BDE-37 16. BDE-75 17. BDE-49 18. BDE-71 19. BDE-47 20. BDE-66 21. BDE-77 22. BDE-100 23. BDE-119 24. BDE-99 25. BDE-116 26. BDE-118 27. BDE-85 28. BDE-155
29. BDE-126 30. BDE-154 31. BDE-153 32. BDE-138 33. BDE-166 34. BDE-183 35. BDE-181 36. BDE-190 37. BDE-208 38. BDE-207 39. BDE-206 40. BDE-209
Conditions
Column Sample
: SH-1614, 15 m, 0.25 mm ID, 0.10 μm (P/N: 227-36265-01)
: 100-300 ppb PBDE PAR Solution 500 ppb decabromodiphenyl ether
Inj. Vol.
: 1 μL splitless (hold 1 min)
Inj. Temp
: 340 °C
Carrier Gas Oven Temp
: He, constant ow, linear velocity 60 cm/sec., 120 °C
: 120 °C (hold 1 min) to 275 °C at 15 °C/min to 300 °C at 5 °C/min (hold 5 min)
Detector
: μ-ECD, 345 °C
Pg C-29
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