GC Columns
SH-5 Amine / SH-35 Amine Dedicated columns for amines and other basic compounds, including alkylamines, diamines, triamines, ethanolamines, and nitrogen-containing heterocyclics.
SH-5 Amine (Low-polarity phase: Crossbond™ 5% diphenyl / 95% dimethyl polysiloxane)
ID
df
Temp. Range
15 m
30 m
0.25 µm
-60 to 300/315 °C
-
227-36282-01
0.25 mm
0.50 µm
-60 to 300/315 °C
227-36323-01
227-36283-01
1.00 µm
-60 to 300/315 °C
227-36323-02
227-36284-01
1.00 µm
-60 to 300/315 °C
-
227-36332-02
0.32 mm
1.50 µm
-60 to 290/305 °C
-
227-36285-01
1.00 µm
-60 to 290/305 °C
-
227-36286-01
0.53 mm
3.00 µm
-60 to 280/295 °C
-
227-36287-01
SH-35 Amine (Mid-polarity phase: Crossbond™ 35% diphenyl / 65% dimethyl polysiloxane)
ID
df
Temp. Range
30 m
0.50 µm
0 to 220 °C
227-36288-01
0.25 mm
1.00 µm
0 to 220 °C
227-36289-01
1.00 µm
0 to 220 °C
227-36290-01
0.32 mm
1.50 µm
0 to 220 °C
227-36291-01
1.00 µm
0 to 220 °C
227-36292-01
0.53 mm
3.00 µm
0 to 220 °C
227-36293-01
Amines & Phenols
Peaks 1. diethylamine 2. pyridine 3. morpholine
9
4
4. phenol 5. aniline 6. 2-chlorophenol 7. diethylenetriamine 8. octylamine 9. 1-methyl-2-pyrrolidinone 10. 2-nitrophenol 11. 2,6-dimethylaniline 12. nicotine 13. 2-nitroaniline
5
3
1 2
13
11
8
Conditions
Column
: SH-5 Amine, 30 m, 0.32 mm ID, 1.00 μm (P/N: 227-36290-01) : 1 μL split injection of miscellaneous amines and phenols in water (split ratio: 25:1)
10
6
Inj. Vol.
7
12
On-column conc. : 22 ng Inj. Temp : 305 °C Oven Temp
: 120 °C to 220 °C at 10 °C/min : Hydrogen, linear velocity 38cm/sec. set at 120 °C
Carrier Gas
Detector Temp FID sensitivity
: 305 °C
: 6.4 × 10 -11 AFS
min. 2
4
6
8
10
Pg C-36
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