Machinery's Handbook, 31st Edition
Heat Treatment of Steel 473 at lower temperatures are preferable because there is less danger of cracking the steel. The temperature of quenching oil baths should range ordinarily between 90 and 130°F (32 and 55°C). A fairly constant temperature may be maintained either by circulating the oil through cooling coils or by using a tank provided with a cold-water jacket. A good quenching oil should possess a flash and fire point sufficiently high to be safe under the conditions used. 350°F (175°C) should be about the minimum point. The spe cific heat of the oil regulates the hardness and toughness of the quenched steel; and the greater the specific heat, the higher will be the hardness produced. Specific heats of quenching oils vary from 0.20 to 0.75, the specific heats of fish, animal, and vegetable oils usually being from 0.2 to 0.4, and of soluble and mineral oils from 0.5 to 0.7. The efficient temperature range for quenching oil is from 90 to 140°F (32 to 60°C). Quenching in Water.— Many carbon tool steels are hardened by immersing them in a bath of fresh water, but water is not an ideal quenching medium. Contact between the water and work and the cooling of the hot steel are impaired by the formation of gas bubbles or an insulating vapor film, especially in holes, cavities, or pockets. The results are uneven cooling and sometimes excessive strains, which may cause the tool to crack; in fact, there is greater danger of cracking in a fresh-water bath than in one containing salt water or brine. In order to secure more even cooling and reduce the danger of cracking, either rock salt (8 or 9 percent) or caustic soda (3 to 5 percent) may be added to the bath to eliminate or prevent the formation of a vapor film or gas pockets, thus promoting rapid early cooling. Brine is commonly used and 3 ⁄ 4 pound of rock salt per gallon (90 gm per liter) of water is equivalent to about 8 percent of salt. Brine is not inherently a more severe or drastic quenching medium than plain water, although it may seem to be because the brine makes better contact with the heated steel, and cooling is more effective. In still-bath quenching, a slow up-and-down movement of the tool is preferable to a violent swishing around. The temperature of water-base quenching baths should preferably be kept around 70°F (21°C), but up to 90 or 100°F (32 to 38°C) is a safe range. The temperature of the hardening bath has a great deal to do with the hardness obtained. The higher the temperature of the quenching water, the more nearly does its effect approach that of oil; and if boiling water is used for quenching, it will have an effect even more gentle than that of oil — in fact, it would leave the steel nearly soft. Parts of irregular shape are sometimes quenched in a water bath that has been warmed somewhat to prevent sudden cooling and cracking. When water is used, it should be “soft” because unsatisfactory results will be obtained with “hard” water. Any contamination of water-base quenching liquids by soap tends to decrease their rate of cooling. A water bath having 1 or 2 inches (2.5 to 5 cm) of oil on the top is sometimes employed to advantage for quenching tools made of high-carbon steel, as the oil through which the work first passes reduces the sudden quenching action of the water. The bath should be amply large to dissipate the heat rapidly, and the temperature should be kept about constant so that successive pieces will be cooled at the same rate. Irregularly shaped parts should be immersed so that the heaviest or thickest section enters the bath first. After immersion, the part to be hardened should be agitated in the bath; the agitation reduces the tendency of the formation of a vapor coating on certain surfaces, and a more uniform rate of cooling is obtained. The work should never be dropped to the bottom of the bath until quite cool. Flush or Local Quenching by Pressure-Spraying: When dies for cold heading, drawing, extruding, etc., or other tools, require a hard working surface and a relatively soft but tough body, the quenching may be done by spraying water under pressure against the interior or other surfaces to be hardened. Special spraying fixtures are used to hold the tool and apply the spray where the hardening is required. The pressure spray prevents the formation of gas pockets previously referred to in connection with the fresh- water quenching bath; hence, fresh water is effective for flush quenching and there is no advantage in using brine.
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